(R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

Base Information

Chemical Name:(R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester
CAS No.:121013-77-2
Molecular Formula:C₁₄H₁₈O₂S
Molecular Weight:250.362
Hs Code.:

Synonyms:(R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

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Chemical Property of (R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

Chemical Property:

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Technology Process of (R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

There total 3 articles about (R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 36240-11-6
(R)-(-)-2-phenylpropionyl chloride

: 121054-78-2
(2S,3R)-Tetrahydro-2-methylthiophen-3-ol

: 121013-77-2
(R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

Guidance literature:: With dmap; In diethyl ether; at 30 ℃; for 3h;

Reference yield:

: 74015-70-6,13679-85-1
4,5-Dihydro-2-methylthiophen-3-(2H)-on

: 121013-77-2
(R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / propan-2-ol / 10 h / 20 °C

2: 88 percent / DMAP / diethyl ether / 3 h / 30 °C

With dmap; sodium tetrahydroborate; In diethyl ether; isopropyl alcohol;

Reference yield:

: 66319-07-1
5-methyl-4-oxotetrahydro-3-thiophencarboxylic acid methyl ester

: 121013-77-2
(R)-2-Phenylpropionsaeure-<(2S,3R)-tetrahydro-2-methylthiophen-3-yl>ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 10percent H₂SO₄ / 3 h / Heating

2: NaBH₄ / propan-2-ol / 10 h / 20 °C

3: 88 percent / DMAP / diethyl ether / 3 h / 30 °C

With dmap; sodium tetrahydroborate; sulfuric acid; In diethyl ether; isopropyl alcohol;