[4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal

Base Information

• Chemical Name: [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal
• CAS No.: 73182-19-1
• Molecular Formula: C₂₃H₂₈N₂O₄S
• Molecular Weight: 428.552

Synonyms:[4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal

Chemical Property of [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal

Chemical Property:

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Technology Process of [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal

There total 2 articles about [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,5-bis(4-methoxyphenyl)-2-mercapto-1H-imidazole (39908-69-5) + Bromoacetaldehyde diethyl acetal (2032-35-1) → [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal (73182-19-1)

Guidance literature:

With sodium; In methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate;

Reference yield:

→ [4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal (73182-19-1)

Guidance literature:

/BRN= 620430/ , NaH, /BRN= 635754/;

Reference yield:

[4,5-bis-(4-methoxy-phenyl)-1H-imidazol-2-ylsulfanyl]-acetaldehyde diethyl acetal (73182-19-1) → 2-(2,2-diethoxy-ethanesulfinyl)-4,5-bis-(4-methoxy-phenyl)-1H-imidazole (73182-20-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; di-isopropyl ether;

upstream raw materials:

4,5-bis(4-methoxyphenyl)-2-mercapto-1H-imidazole

Bromoacetaldehyde diethyl acetal

Downstream raw materials:

2-(2,2-diethoxy-ethanesulfinyl)-4,5-bis-(4-methoxy-phenyl)-1H-imidazole

2-(2,2-diethoxy-ethanesulfonyl)-4,5-bis-(4-methoxy-phenyl)-1H-imidazole

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