(R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

Base Information

Chemical Name:(R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde
CAS No.:219561-54-3
Molecular Formula:C₂₅H₂₃NO₃
Molecular Weight:385.463
Hs Code.:

Synonyms:(R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

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Chemical Property of (R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

Chemical Property:

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Technology Process of (R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

There total 1 articles about (R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4S,5R)-3-{1-[(E)-Cyclohexyliminomethyl]-1-methyl-2-phenyl-ethyl}-4,5-diphenyl-oxazolidin-2-one

: (S)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

: 219561-54-3
(R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; Yield given; Yields of byproduct given;
DOI:10.1021/ja9823518

Reference yield:

: 219561-54-3
(R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

: 17350-84-4
(R)-2-amino-2-methyl-3-phenylpropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaClO₂, NaH₂PO₄

2: H₂ / Pd(OH)2

With sodium chlorite; sodium dihydrogenphosphate; hydrogen; palladium dihydroxide;
DOI:10.1021/ja9823518

Reference yield:

: 219561-54-3
(R)-2-Methyl-2-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-3-phenyl-propionaldehyde

: 219561-11-2
2-Methyl-2-{3-[(R)-1-methyl-1-((4S,5R)-2-oxo-4,5-diphenyl-oxazolidin-3-yl)-2-phenyl-ethyl]-oxaziridin-2-yl}-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 4 A molecular sieves / benzene / 26 h / Heating

2: m-CPBA, 10 percent NaHCO₃, O₂ / CH₂Cl₂; toluene / 0.5 h / -78 °C

With 4 A molecular sieve; oxygen; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; benzene;
DOI:10.1021/ja9823518