benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

Base Information

Chemical Name:benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate
CAS No.:1267638-65-2
Molecular Formula:C₅₂H₇₂N₈O₆
Molecular Weight:905.194
Hs Code.:

benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

Synonyms:benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

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Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

There total 4 articles about benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1267638-49-2
benzyl ((4R)-4-amino-5-[(4-((2-tert-butyl-6-methoxyquinolin-8-yl)amino)pentyl)amino]-5-oxopentyl)carbamate

: 530-62-1
1,1'-carbonyldiimidazole

: 655250-09-2
N₈-(4-amino-1-methylpentyl)-2-tert-butyl-6-methoxy-8-quinolinamine

: 1267638-65-2
benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

Guidance literature:: benzyl ((4R)-4-amino-5-[(4-((2-tert-butyl-6-methoxyquinolin-8-yl)amino)pentyl)amino]-5-oxopentyl)carbamate; 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 0.5h;

N₈-(4-amino-1-methylpentyl)-2-tert-butyl-6-methoxy-8-quinolinamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1016/j.bmc.2010.11.036

Reference yield:

: 1267638-34-5
benzyl [(4R)-4-[(tert-butoxycarbonyl)amino]-5-((4-[(2-tert-butyl-6-methoxyquinolin-8-yl)-amino]pentyl)amino)-5-oxopentyl]-carbamate

: 1267638-65-2
benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; methanol / 0.75 h / 20 °C

2.1: dichloromethane / 0.5 h / 20 °C

2.2: 5 h / 20 °C

With hydrogenchloride; methanol; In dichloromethane;
DOI:10.1016/j.bmc.2010.11.036

Reference yield:

: 2480-93-5,16937-92-1
(R)-Nδ-benzyloxycarbonyl-Nα-(tert-butoxycarbonyl)-ornithine

: 1267638-65-2
benzyl {(4R)-5-({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}amino)-4-[({4-[(2-tert-butyl-6-methoxyquinolin-8-yl)amino]pentyl}carbamoyl)amino]-5-oxopentyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropyl-carbodiimide / dichloromethane / 4 h / 0 - 20 °C

2.1: hydrogenchloride; methanol / 0.75 h / 20 °C

3.1: dichloromethane / 0.5 h / 20 °C

3.2: 5 h / 20 °C

With hydrogenchloride; methanol; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.bmc.2010.11.036