2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

Base Information

Chemical Name:2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine
CAS No.:135824-28-1
Molecular Formula:C₂₇H₄₄N₂O₅SeSi₂
Molecular Weight:611.788
Hs Code.:

Synonyms:2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

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Chemical Property of 2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

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Technology Process of 2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

There total 1 articles about 2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1666-13-3
diphenyl diselenide

: 129801-93-0
2',3'-bis-O-(tert-butyldimethylsilyl)-O²,5'-cyclouridine

: 135824-28-1
2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

Guidance literature:: With sodium tetrahydroborate; Yield given. Multistep reaction; 1) THF, EtOH, 10 min., room temp., 2) THF, 2 h, room temp.;
DOI:10.1021/jo00018a038

Reference yield: 100.0%

: 135824-28-1
2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

: 142794-50-1
C₂₇H₄₄N₂O₆SeSi₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jo00018a038

Reference yield:

: 135824-28-1
2',3'-bis-O-(tert-butyldimethylsilyl)-5'-deoxy-5'-(phenylseleno)uridine

: Benzoic acid (S)-1-[(2R,3R,4R,5R)-3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-3-chloro-but-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: m-CPBA / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 56 percent / (Bu₃Sn)2 / benzene / Irradiation

With bis(tri-n-butyltin); 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1016/0040-4020(96)00483-8