C₃₄H₅₀INO₁₀Si

Base Information

Chemical Name:C₃₄H₅₀INO₁₀Si
CAS No.:1617543-85-7
Molecular Formula:C₃₄H₅₀INO₁₀Si
Molecular Weight:787.762
Hs Code.:

C<sub>34</sub>H<sub>50</sub>INO<sub>10</sub>Si

Synonyms:C₃₄H₅₀INO₁₀Si

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Chemical Property of C₃₄H₅₀INO₁₀Si

Chemical Property:

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Technology Process of C₃₄H₅₀INO₁₀Si

There total 5 articles about C₃₄H₅₀INO₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1617543-84-6
C₂₃H₃₀INO₁₀

: 127016-36-8
8-iodo-1-(trimethylsilyl)-1-octyne

: 1617543-85-7
C₃₄H₅₀INO₁₀Si

Guidance literature:: C₂₃H₃₀INO₁₀; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.166667h;

8-iodo-1-(trimethylsilyl)-1-octyne; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;
DOI:10.1016/j.tet.2014.05.108

Reference yield:

: 1617543-82-4
C₁₈H₂₃ClINO₆

: 1617543-85-7
C₃₄H₅₀INO₁₀Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide / acetone / Reflux

2.1: sodium hydride / mineral oil; tetrahydrofuran

2.2: 20 °C

3.1: N,N-dimethyl-formamide; mineral oil / 0.17 h / 20 °C

3.2: 20 °C

With sodium hydride; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1016/j.tet.2014.05.108

Reference yield:

: 1617543-75-5
C₁₂H₁₂INO₆

: 1617543-85-7
C₃₄H₅₀INO₁₀Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 20 °C

1.2: 6 h / 20 °C

2.1: sodium iodide / acetone / Reflux

3.1: sodium hydride / mineral oil; tetrahydrofuran

3.2: 20 °C

4.1: N,N-dimethyl-formamide; mineral oil / 0.17 h / 20 °C

4.2: 20 °C

With sodium hydride; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1016/j.tet.2014.05.108