Technology Process of C8H6BrNO2
There total 6 articles about C8H6BrNO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: aluminum (III) chloride / 3 h / 160 °C / Inert atmosphere
3: sodium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
4: pyridine; hydroxylamine hydrochloride / 6 h / 130 °C / Inert atmosphere
5: N,N`-dimethylethylenediamine; sodium t-butanolate; copper(l) iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
6: boron tribromide / dichloromethane / 0 °C / Inert atmosphere
With
pyridine; aluminum (III) chloride; copper(l) iodide; hydroxylamine hydrochloride; boron tribromide; sodium carbonate; sodium t-butanolate; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aluminum (III) chloride / 3 h / 160 °C / Inert atmosphere
2: sodium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
3: pyridine; hydroxylamine hydrochloride / 6 h / 130 °C / Inert atmosphere
4: N,N`-dimethylethylenediamine; sodium t-butanolate; copper(l) iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
5: boron tribromide / dichloromethane / 0 °C / Inert atmosphere
With
pyridine; aluminum (III) chloride; copper(l) iodide; hydroxylamine hydrochloride; boron tribromide; sodium carbonate; sodium t-butanolate; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;