diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

Base Information

Chemical Name:diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate
CAS No.:1351663-34-7
Molecular Formula:C₂₄H₂₇BrNO₄P
Molecular Weight:504.36
Hs Code.:

Synonyms:diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

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Chemical Property of diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

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Technology Process of diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

There total 3 articles about diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1351663-32-5
4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzyl alcohol

: 122-52-1
triethyl phosphite

: 1351663-34-7
diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

Guidance literature:: With iodine; at 0 - 20 ℃;
DOI:10.1002/ejoc.201100821

Reference yield:

: 1351663-31-4
4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzaldehyde

: 1351663-34-7
diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 0 - 20 °C

2: iodine / 0 - 20 °C

With sodium tetrahydroborate; iodine; In ethanol;
DOI:10.1002/ejoc.201100821

Reference yield:

: 87755-82-6
4-[N-phenyl-N-(4-methoxyphenyl)amino]benzaldehyde

: 1351663-34-7
diethyl 4-[N-(4-bromophenyl)-N-(4-methoxyphenyl)amino]benzylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / -5 - 0 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 0 - 20 °C

3: iodine / 0 - 20 °C

With sodium tetrahydroborate; N-Bromosuccinimide; iodine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100821