2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

Base Information

Chemical Name:2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone
CAS No.:169566-48-7
Molecular Formula:C₇₀H₆₄O₁₀
Molecular Weight:1065.27
Hs Code.:

Synonyms:2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

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Chemical Property of 2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

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Technology Process of 2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

There total 3 articles about 2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 169566-48-7
2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

Guidance literature:: Multi-step reaction with 3 steps

1: calcium sulfate; trimethylsilyl trifluoromethanesulfonate / acetonitrile; dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

3: sodium hydroxide / water; ethanol / 24 °C / Reflux

With calcium sulfate; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acs.jmedchem.6b01134

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 169566-48-7
2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

Guidance literature:: Multi-step reaction with 3 steps

1: calcium sulfate; trimethylsilyl trifluoromethanesulfonate / acetonitrile; dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

3: sodium hydroxide / water; ethanol / 24 °C / Reflux

With calcium sulfate; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acs.jmedchem.6b01134

Reference yield:

: 1309438-45-6
4,6-bis-hydroxy-3-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-2-hydroxyacetophenone

: 169566-48-7
2'-hydroxy-3'-C-β-D-(2,3,4,6-tetra-O-benzylglucopyranosyl)-4,4',6'-tribenzyloxychalcone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

2: sodium hydroxide / water; ethanol / 24 °C / Reflux

With potassium carbonate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.6b01134