(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

Base Information

Chemical Name:(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside
CAS No.:1352427-79-2
Molecular Formula:C₆₈H₅₄O₁₉
Molecular Weight:1175.17
Hs Code.:

Synonyms:(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

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Chemical Property of (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

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Technology Process of (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

There total 3 articles about (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 853308-55-1
C₃₇H₃₂O₁₀

: 1352427-79-2
(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

: 627466-98-2
2,3,4,6-tetra-O-benzoyl-α,β-D-mannospyranose

: allyl-2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃; for 0.166667h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo202335n

Reference yield: 38.0%

: 65236-82-0,65236-87-5,92761-43-8,106930-83-0,134677-35-3
1,2-O-(α-methoxybenzylidene)-3,4,6-tri-O-benzoyl-β-D-mannopyranose

: 3947-62-4,6207-76-7,10343-06-3,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1
2,3,4,6-tetra-O-acetyl-D-mannopyranose

: 6605-40-9,14315-82-3,32849-03-9,34820-00-3,39681-87-3,80245-01-8,80245-02-9,93768-42-4,97100-67-9
methyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

: 439-01-0,3825-18-1,4163-39-7,4163-40-0,147384-47-2
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl fluoride

: (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-acetyl-β-D-mannopyranoside

: 1352278-39-7
(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 1352427-79-2
(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃; for 0.0833333h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo202335n

Reference yield:

: 3254-16-8,4435-05-6,19189-54-9,29748-21-8,50801-29-1,64727-26-0,64727-27-1,65338-02-5,67672-68-8,78418-55-0,80877-03-8,103002-27-3,103002-29-5,132562-62-0
3,4,6-tri-O-acetyl-1,2-O-(1-methoxyethylidene)-β-D-mannopyranose

: 1352427-79-2
(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-2,3,4,6-tetra-O-benzoyl-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: ytterbium(III) triflate / dichloromethane / 5.5 h / 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -30 °C / Inert atmosphere

With boron trifluoride diethyl etherate; ytterbium(III) triflate; In dichloromethane;
DOI:10.1021/jo202335n