Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester
CAS No.:130718-47-7
Molecular Formula:C₃₃H₃₄O₉S
Molecular Weight:606.694
Hs Code.:

Synonyms:Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

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Chemical Property of Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

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Technology Process of Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

There total 1 articles about Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: tetrabutylammonium salt of triphenylmethanethiol

: 572-10-1,4451-35-8,4451-36-9,14227-52-2,14227-87-3,14227-88-4,14257-40-0,17081-03-7,19186-60-8,57237-01-1,65982-17-4,65982-18-5,65982-19-6,66966-08-3,144299-57-0
2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl chloride

: 130718-47-7
Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

Guidance literature:: In toluene; for 12h; Ambient temperature;
DOI:10.1016/S0040-4039(00)97491-4

Reference yield: 100.0%

: 130718-47-7
Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

: 130718-48-8
triphenylmethyl 1-thio-α-D-galactopyranoside

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1016/S0040-4039(00)97491-4

Reference yield:

: 130718-47-7
Acetic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-tritylsulfanyl-tetrahydro-pyran-3-yl ester

: (4aR,6R,7R,8R,8aR)-2-Phenyl-6-tritylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOMe / methanol

2: HBF₄ / diethyl ether; dimethylformamide

With tetrafluoroboric acid; sodium methylate; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)97491-4