[(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

Chemical Name:[(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester
CAS No.:144877-27-0
Molecular Formula:C₂₃H₃₉NO₇
Molecular Weight:441.565
Hs Code.:

[(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Synonyms:[(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Suppliers and Price of [(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

There total 2 articles about [(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 144877-25-8
Carbonic acid 2,5-dioxo-pyrrolidin-1-yl ester (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

: 300572-82-1
3-azido-3-deoxy-1,2;5,6-di-O-isopropylidene-α-D-allofuranose

: 144877-27-0
[(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1039/c39920001308

Reference yield:

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 144877-27-0
[(3aR,5S,6R,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl]-carbamic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / acetonitrile / 4 h / 23 °C

2: 80 percent / H₂, Et₃N / 10percent Pd/C / tetrahydrofuran

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c39920001308