4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

Base Information

• Chemical Name: 4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine
• CAS No.: 93118-47-9
• Molecular Formula: C₂₃H₂₆Cl₂N₄O₇S
• Molecular Weight: 573.454

Synonyms:4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

Chemical Property of 4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

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Technology Process of 4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine

There total 1 articles about 4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine (88150-50-9) + 3,4-dimethoxy-1,2,5-thiadiazole-1-oxide (78441-23-3) → 4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine (93118-47-9)

Guidance literature:

In methanol; for 18h; Heating;

DOI:10.1021/jm00123a009

Reference yield: 49.0%

4-(2,3-Dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-2-<<2-<(3-methoxy-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-6-methyl-1,4-dihydropyridine (93118-47-9) → 2-<<2-<(3-Amino-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine (93118-33-3)

Guidance literature:

With ammonia; for 1h; Ambient temperature;

DOI:10.1021/jm00123a009

upstream raw materials:

2-[(2-aminoethoxy)methyl]-4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

3,4-dimethoxy-1,2,5-thiadiazole-1-oxide

Downstream raw materials:

2-<<2-<(3-Amino-1-oxo-1,2,5-thiadiazol-4-yl)amino>ethoxy>methyl>-4-(2,3-dichlorophenyl)-3-(ethoxycarbonyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine

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