((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

Base Information

Chemical Name:((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate
CAS No.:1206481-27-7
Molecular Formula:C₁₈H₂₄O₅
Molecular Weight:320.386
Hs Code.:

Synonyms:((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

Suppliers and Price of ((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

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Technology Process of ((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

There total 1 articles about ((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1206481-26-6
(2R,3S,4S)-2,3,4-trihydroxyhex-5-enyl pivalate

: 1125-88-8
benzaldehyde dimethyl acetal

: 1206481-27-7
((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.024

Reference yield: 57.0%

: 1206481-27-7
((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

: 2746-25-0
p-Methoxybenzyl bromide

: 1206481-28-8
((2S,4R,5S,6S)-5-(4-methoxybenzyloxy)-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate

Guidance literature:: ((2S,4R,5S,6S)-5-hydroxy-2-phenyl-6-vinyl-1,3-dioxan-4-yl)methyl pivalate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -5 ℃; Inert atmosphere;

p-Methoxybenzyl bromide; In N,N-dimethyl-formamide; mineral oil; at -5 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.024