(2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Base Information

• Chemical Name: (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester
• CAS No.: 204061-12-1
• Molecular Formula: C₃₇H₄₄N₂O₅Si
• Molecular Weight: 624.852

Synonyms:(2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Chemical Property of (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Chemical Property:

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Technology Process of (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

There total 4 articles about (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) + {2-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-ethyl}-carbamic acid benzyl ester → (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester (204061-12-1)

Guidance literature:

With triethylamine; In dichloromethane; Yield given; Ambient temperature;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

2-(((benzyloxy)carbonyl)amino)ethyl 1-methanesulfonate (134307-72-5) → (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester (204061-12-1)

Guidance literature:

Multi-step reaction with 4 steps

1: NaBr / dimethylformamide

2: K₂CO₃ / CHCl₃

3: Et₃N, DMAP / CH₂Cl₂

4: Et₃N / CH₂Cl₂ / Ambient temperature

With dmap; potassium carbonate; triethylamine; sodium bromide; In dichloromethane; chloroform; N,N-dimethyl-formamide;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

benzyl N-(2-bromoethyl)carbamate (53844-02-3) → (2-Benzyloxycarbonylamino-ethyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester (204061-12-1)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃ / CHCl₃

2: Et₃N, DMAP / CH₂Cl₂

3: Et₃N / CH₂Cl₂ / Ambient temperature

With dmap; potassium carbonate; triethylamine; In dichloromethane; chloroform;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

upstream raw materials:

benzyl chloroformate

benzyl N-(2-bromoethyl)carbamate

2-(((benzyloxy)carbonyl)amino)ethyl 1-methanesulfonate

Downstream raw materials:

{2-[Benzyloxycarbonyl-(3-hydroxy-propyl)-amino]-ethyl}-carbamic acid benzyl ester

{2-[(3-Azido-propyl)-benzyloxycarbonyl-amino]-ethyl}-carbamic acid benzyl ester

C₅₁H₇₆N₄O₆

C₅₂H₇₈N₄O₆

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