Technology Process of C19H20F2N6O
There total 6 articles about C19H20F2N6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Berger Minigram; column: Daicel IC;
In
methanol; carbon dioxide; diethylamine;
at 40 ℃;
under 75007.5 Torr;
Purification / work up;
Resolution of racemate;
- Guidance literature:
-
With
Diacel IC;
In
methanol; carbon dioxide; diethylamine;
at 40 ℃;
under 75007.5 Torr;
Resolution of racemate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / ethanol; mineral oil / 0.75 h / 140 °C / Inert atmosphere; Microwave irradiation
2.1: acetyl chloride; methanol / toluene / 12 h / 0 - 20 °C
2.2: 0.5 h / 0 - 20 °C
2.3: pH 1
3.1: 1 h / 175 °C / Microwave irradiation
4.1: Berger Minigram; column: Daicel IC / diethylamine; carbon dioxide; methanol / 40 °C / 75007.5 Torr / Resolution of racemate
With
methanol; sodium hydride; acetyl chloride;
In
methanol; ethanol; carbon dioxide; diethylamine; toluene; mineral oil;