diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate

Base Information

Chemical Name:diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate
CAS No.:102821-34-1
Molecular Formula:C₂₁H₂₈O₉
Molecular Weight:424.448
Hs Code.:

Synonyms:diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate

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Technology Process of diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate

There total 2 articles about diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54130-89-1
2,6-dimethoxy-4-methyl-benzoic acid methyl ester

: 102821-34-1
diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate

Guidance literature:: Multi-step reaction with 2 steps

1: 61.4 percent / N-bromosuccinimide, di-t-butyl peroxyde / CCl₄ / 30 h / Heating

2: 1) NaH / 1) toluene, 0 deg C, 20 min, 2) toluene, r.t., 48 h

With N-Bromosuccinimide; di-tert-butyl peroxide; sodium hydride; In tetrachloromethane;
DOI:10.1016/S0040-4020(01)96675-X

Reference yield:

: 1115-30-6
diethyl acetylsuccinate

: 102821-33-0
methyl-4-bromomethyl-2,6-dimethoxy benzoate

: 102821-34-1
diethyl-2-acetyl-2-(4-carbomethoxy-3,5-dimethoxyphenylmethyl)butandioate

Guidance literature:: With sodium hydride; Multistep reaction; 1) toluene, 0 deg C, 20 min, 2) toluene, r.t., 48 h;
DOI:10.1016/S0040-4020(01)96675-X