(S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

Base Information

Chemical Name:(S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde
CAS No.:138436-32-5
Molecular Formula:C₂₂H₃₈O₅Si
Molecular Weight:410.626
Hs Code.:

Synonyms:(S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

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Chemical Property of (S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

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Technology Process of (S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

There total 13 articles about (S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2-(4-methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propan-1-ol

: 138436-32-5
(R)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

: 138436-32-5
(S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

Guidance literature:: With phosgene; dimethyl sulfoxide; diisopropylamine; Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)00351-8

Reference yield: 92.0%

: 2-(4-methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propan-1-ol

: 138436-32-5
(R)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

: 138436-32-5
(S)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

Guidance literature:: With phosgene; dimethyl sulfoxide; diisopropylamine; Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)00351-8

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 138436-32-5
(R)-2-(4-Methoxy-benzyloxymethoxymethyl)-3-triisopropylsilanyloxy-propionaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-lutidine / CH₂Cl₂ / 0 °C

2: KOH / methanol

3: 92 percent / EtN(iPr)2 / CH₂Cl₂ / 0 deg C to r.t.

4: 1) O₃, 2) Me₂S

With 2,6-dimethylpyridine; potassium hydroxide; dimethylsulfide; ozone; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1016/0040-4039(91)80449-G