1,4-Diaminobutane-15N2 dihydrochloride

Base Information

Chemical Name:1,4-Diaminobutane-15N2 dihydrochloride
CAS No.:2747-92-4
Molecular Formula:C4H12 N2 . 2 Cl H
Molecular Weight:163.09
Hs Code.:
European Community (EC) Number:685-861-6
DSSTox Substance ID:DTXSID00583888
Mol file:2747-92-4.mol

Synonyms:1,4-Diaminobutane-15N2 dihydrochloride;2747-92-4;butane-1,4-di(15N2)amine;dihydrochloride;DTXSID00583888;1,4-Diaminobutane-15N2 dihydrochloride, 98 atom % 15N;Butane-1,4-(~15~N_2_)diamine--hydrogen chloride (1/2)

Suppliers and Price of 1,4-Diaminobutane-15N2 dihydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,4-DIAMINOBUTANE-15N2 DIHYDROCHLORIDE 95.00%
5MG
$ 498.64

Total 1 raw suppliers

Chemical Property of 1,4-Diaminobutane-15N2 dihydrochloride

Chemical Property:

Melting Point:280 °C (dec.)(lit.)
PSA：52.04000
LogP:2.68860
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:162.0474736
Heavy Atom Count:8
Complexity:17.5

Purity/Quality:

97% ^*data from raw suppliers

1,4-DIAMINOBUTANE-15N2 DIHYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(CCN)CN.Cl.Cl
Isomeric SMILES:C(CC[15NH2])C[15NH2].Cl.Cl

Technology Process of 1,4-Diaminobutane-15N2 dihydrochloride

There total 3 articles about 1,4-Diaminobutane-15N2 dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 93827-87-3
15N-(benzyloxycarbonyl)putrescine

: 2747-92-4
[1,4-15N₂]-putrescine dihydrochloride

: C₂₃H₂₇N⁽¹⁵⁾N₂O₄

Guidance literature:: With potassium fluoride; In acetonitrile; for 2h; Heating;
DOI:10.1248/cpb.32.3428

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 53510-88-6
potassium phthalimide-15N

: 2747-92-4
[1,4-15N₂]-putrescine dihydrochloride

Guidance literature:: With hydrogenchloride; acetic acid; Yield given. Multistep reaction; 1) DMF, 90 deg C, 3 h; 12 deg C, 3 d;
DOI:10.1248/cpb.32.3428