O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

Base Information

Chemical Name:O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate
CAS No.:1265174-91-1
Molecular Formula:C₂₂H₁₄F₄N₄O₂S
Molecular Weight:474.438
Hs Code.:

Synonyms:O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

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Chemical Property of O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

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Technology Process of O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

There total 4 articles about O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1181214-75-4
4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)aniline

: 42908-73-6
4-fluorophenyl chlorothionoformate

: 1265174-91-1
O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 1181214-76-5
3-(4-nitrophenyl)-1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazole

: 1265174-91-1
O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on activated charcoal / ethanol

2: triethylamine / tetrahydrofuran / 2 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol;

Reference yield:

: 1181214-77-6
1-(4-nitrobenzylidene)-2-(4-(trifluoromethoxy)phenyl)hydrazine

: 1265174-91-1
O-4-fluorophenyl 4-(1-(4-(trifluoromethoxy)phenyl)-1H-1,2,4-triazol-3-yl)phenylcarbamothioate

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; dimethylsulfide / dichloromethane / 2 h / -20 - 20 °C / Inert atmosphere

2: triethylamine / ethanol / 2 h / Reflux

3: hydrogen / palladium on activated charcoal / ethanol

4: triethylamine / tetrahydrofuran / 2 h / 20 °C

With N-Bromosuccinimide; dimethylsulfide; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;