2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

Base Information

Chemical Name:2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)
CAS No.:103726-05-2
Molecular Formula:C₃₆H₃₇O₁₅PS₂
Molecular Weight:804.787
Hs Code.:

Synonyms:2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

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Chemical Property of 2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

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Technology Process of 2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

There total 3 articles about 2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50651-75-7
silver dibenzylphosphate

: 103726-04-1
2,3-di-O-benzoyl-4,6-di-O-mesyl-α-D-glucopyranosyl bromide

: 103726-05-2
2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: With calcium sulfate; In benzene; for 1.5h; Heating;
DOI:10.1016/S0008-6215(00)90641-4

Reference yield:

: 22435-33-2
methyl-2,3-di-O-benzoyl-4,6-di-O-mesyl-α-D-glucopyranoside

: 103726-05-2
2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / conc. sulphuric acid / 24 h / 20 °C

2: 89 percent / 45percent hydrogen bromide / CH₂Cl₂; acetic acid / 2 h / 20 °C

3: 71 percent / Drierite / benzene / 1.5 h / Heating

With calcium sulfate; sulfuric acid; hydrogen bromide; In dichloromethane; acetic acid; benzene;
DOI:10.1016/S0008-6215(00)90641-4

Reference yield:

: 34980-19-3
1-O-acetyl-2,3-di-O-benzoyl-4,6-di-O-mesyl-α-D-glucopyranose

: 103726-05-2
2,3-di-O-benzoyl-4,6-di-O-mesyl-β-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 45percent hydrogen bromide / CH₂Cl₂; acetic acid / 2 h / 20 °C

2: 71 percent / Drierite / benzene / 1.5 h / Heating

With calcium sulfate; hydrogen bromide; In dichloromethane; acetic acid; benzene;
DOI:10.1016/S0008-6215(00)90641-4