Technology Process of C43H31N3
There total 3 articles about C43H31N3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine;
In
toluene;
at 90 ℃;
for 6h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / toluene; ethanol / 36 h / 90 °C
2: sodium hydroxide / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 12 h / 70 °C / Inert atmosphere
3: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 90 °C / Inert atmosphere
With
toluene-4-sulfonic acid; sodium hydroxide; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine;
In
tetrahydrofuran; ethanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / palladium diacetate / toluene / 4 h / 90 °C / Inert atmosphere
2: toluene-4-sulfonic acid / toluene; ethanol / 36 h / 90 °C
3: sodium hydroxide / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / 12 h / 70 °C / Inert atmosphere
4: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 90 °C / Inert atmosphere
With
potassium tert-butylate; toluene-4-sulfonic acid; sodium hydroxide; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; palladium diacetate;
In
tetrahydrofuran; ethanol; water; toluene;