3-(cyclohexylamino)thiocinnamaldehyde

Base Information

Chemical Name:3-(cyclohexylamino)thiocinnamaldehyde
CAS No.:124413-36-1
Molecular Formula:C₁₅H₁₉NS
Molecular Weight:245.389
Hs Code.:

Synonyms:3-(cyclohexylamino)thiocinnamaldehyde

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Chemical Property of 3-(cyclohexylamino)thiocinnamaldehyde

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Technology Process of 3-(cyclohexylamino)thiocinnamaldehyde

There total 2 articles about 3-(cyclohexylamino)thiocinnamaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 3-cyclohexylamino-3-phenylallylidene-(N,N-dimethyl)ammonium phosphorodichloridate

: 124413-36-1
3-(cyclohexylamino)thiocinnamaldehyde

Guidance literature:: With sodium hydrogensulfide; In methanol; for 1h; Ambient temperature;
DOI:10.1039/P19890001241

Reference yield:

: 124413-78-1
α-(cyclohexylamino)styrene

: 124413-36-1
3-(cyclohexylamino)thiocinnamaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / POCl₃ / 1) 35 deg C, 4 h, 2) r.t., 20 h

2: 81 percent / 2M NaHS / methanol / 1 h / Ambient temperature

With sodium hydrogensulfide; trichlorophosphate; In methanol;
DOI:10.1039/P19890001241