Technology Process of C35H29N3O
There total 2 articles about C35H29N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
water; tert-butyl alcohol;
at 20 - 80 ℃;
DOI:10.1021/ja1102844
- Guidance literature:
-
Multi-step reaction with 2 steps
1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 18 h / 20 °C
2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 - 80 °C
With
imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate;
In
methanol; water; tert-butyl alcohol;
DOI:10.1021/ja1102844
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium azide; trifluoroacetic acid / 0 °C
1.2: 0.5 h / 0 °C
2.1: ammonium formate; zinc / methanol / 15 h / 20 °C / Inert atmosphere
With
sodium azide; ammonium formate; trifluoroacetic acid; zinc;
In
methanol;
DOI:10.1021/ja1102844