[6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

Base Information

Chemical Name:[6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate
CAS No.:181024-58-8
Molecular Formula:C₃₈H₄₃Cl₃N₄O₁₅
Molecular Weight:902.136
Hs Code.:

[6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

Synonyms:[6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

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Chemical Property of [6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

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Technology Process of [6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

There total 3 articles about [6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 545-06-2
trichloroacetonitrile

: 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-D-glucopyranose

: 181024-58-8
[6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1016/S0968-0896(99)00113-3

Reference yield:

: (2R,3S,4S,5R,6R)-5-Acetoxy-6-((2R,3S,4R,5R)-6-acetoxy-2-acetoxymethyl-5-azido-4-benzyloxy-tetrahydro-pyran-3-yloxy)-4-benzyloxy-3-(4-oxo-pentanoyloxy)-tetrahydro-pyran-2-carboxylic acid methyl ester

: 181024-58-8
[6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-levulinyl-α-L-idopyranosyluronate)-β-D-glucopyranosyl] trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / BnNH₂ / diethyl ether / 20 °C

2: 81 percent / K₂CO₃ / CH₂Cl₂ / 5 h / 20 °C

With potassium carbonate; benzylamine; In diethyl ether; dichloromethane; 1: Deacetylation / 2: Substitution;
DOI:10.1016/S0968-0896(99)00113-3