N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Base Information

Chemical Name:N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole
CAS No.:158407-19-3
Molecular Formula:C₆₂H₇₅N₅O₈
Molecular Weight:1018.31
Hs Code.:

Synonyms:N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

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Chemical Property of N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

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Technology Process of N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

There total 6 articles about N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 129063-53-2
cis,cis-1,3,5-tripropylcyclohexane-1,3,5-tricarboxylic acid imide chloride

: 158407-18-2
N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-diaminocarbazole

: 158407-19-3
N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Guidance literature:: With pyridine; dmap; for 16h; Heating;
DOI:10.1021/ja00099a003

Reference yield:

: 158407-15-9
methyl 4’-iodo-[1,1’-biphenyl]-4-carboxylate

: 158407-19-3
N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / K₂CO₃, Cu / xylene / 48 h / Heating

2: 97 percent / HOAc, conc. HNO₃ / 5 h / 70 °C

3: H₂ / 10percent Pd/C / tetrahydrofuran / 26 h

4: 58 percent / DMAP, pyridine / 16 h / Heating

With pyridine; dmap; hydrogen; nitric acid; copper; potassium carbonate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; xylene;
DOI:10.1021/ja00099a003

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 158407-19-3
N-(4-(4'-(methoxycarbonyl)phenyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tripropyl-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / K₂CO₃, Cu / xylene / 48 h / Heating

2: 97 percent / HOAc, conc. HNO₃ / 5 h / 70 °C

3: H₂ / 10percent Pd/C / tetrahydrofuran / 26 h

4: 58 percent / DMAP, pyridine / 16 h / Heating

With pyridine; dmap; hydrogen; nitric acid; copper; potassium carbonate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; xylene;
DOI:10.1021/ja00099a003