Cyclopentanecarboxamide, 3-hydroxy-4-(hydroxymethyl)-, (1alpha,3beta,4alpha)- (9CI)

Base Information

Chemical Name:Cyclopentanecarboxamide, 3-hydroxy-4-(hydroxymethyl)-, (1alpha,3beta,4alpha)- (9CI)
CAS No.:23722-87-4
Molecular Formula:C₇H₁₃NO₃
Molecular Weight:159.185
Hs Code.:
Mol file:23722-87-4.mol

Synonyms:Cyclopentanecarboxamide,3-hydroxy-4-(hydroxymethyl)-, stereoisomer (8CI)

Suppliers and Price of Cyclopentanecarboxamide, 3-hydroxy-4-(hydroxymethyl)-, (1alpha,3beta,4alpha)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Cyclopentanecarboxamide, 3-hydroxy-4-(hydroxymethyl)-, (1alpha,3beta,4alpha)- (9CI)

Chemical Property:

PSA：83.55000
LogP:-0.44860

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopentanecarboxamide, 3-hydroxy-4-(hydroxymethyl)-, (1alpha,3beta,4alpha)- (9CI)

There total 3 articles about Cyclopentanecarboxamide, 3-hydroxy-4-(hydroxymethyl)-, (1alpha,3beta,4alpha)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 23722-85-2,99295-42-8
(+/-)methyl (1β,3β,4β)-2-acetoxy-4-carbamoylcyclopentanecarboxylate

: 23722-87-4,99295-43-9
(+/-)-(1β,3β,4β)-3-hydroxy-4-(hydroxymethyl)lcyclopentanecarboxamide

Guidance literature:: With lithium borohydride; In tetrahydrofuran; for 0.333333h; Heating;
DOI:10.1139/v85-464

Reference yield:

: 99236-92-7
(+/-)-(1β,3β,4β)-4-acetoxy-4-carbamoylcyclopentanedicarboxylic acid

: 23722-87-4,99295-43-9
(+/-)-(1β,3β,4β)-3-hydroxy-4-(hydroxymethyl)lcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 79.1 percent / methanol

2: 81 percent / LiBH₄ / tetrahydrofuran / 0.33 h / Heating

With lithium borohydride; In tetrahydrofuran; methanol;
DOI:10.1139/v85-464

Reference yield:

: 23722-87-4,99295-43-9
(+/-)-(1β,3α,4β)-3-Hydroxy-4-(hydroxymethyl)cyclopentanecarboxamide

Guidance literature:: (+-)-2trans-Acetoxy-4cis-carbamoyl-cyclopentan-carbonsaeure-(1ref)-methylester, LiBH4 in THF;
DOI:10.1016/S0040-4039(01)88129-6