(2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

Base Information

Chemical Name:(2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane
CAS No.:156604-31-8
Molecular Formula:C₂₂H₃₅N₃O₆
Molecular Weight:437.536
Hs Code.:

(2S)-N<sup>4</sup>-benzyloxycarbonyl-N<sup>1</sup>,N<sup>2</sup>-di-tert-butoxycarbonyl-1,2,4-triaminobutane

Synonyms:(2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

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Technology Process of (2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

There total 14 articles about (2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 868069-39-0
(2S)-N⁴-benzyloxycarbonyl-1,2,4-triaminobutane

: 24424-99-5
di-tert-butyl dicarbonate

: 156604-31-8
(2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 24h;
DOI:10.1055/s-2005-869989

Reference yield: 52.0%

: 24424-99-5
di-tert-butyl dicarbonate

: benzyl tert-butyl (4-aminobutane-1,3-diyl)-(S)-dicarbamate

: 156604-31-8
(2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

Guidance literature:: With trimethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 868069-38-9
(2S)-N⁴-benzyloxycarbonyl-2,4-diaminobutanamide

: 156604-31-8
(2S)-N⁴-benzyloxycarbonyl-N¹,N²-di-tert-butoxycarbonyl-1,2,4-triaminobutane

Guidance literature:: Multi-step reaction with 2 steps

1: BH₃*THF / tetrahydrofuran / 5 h / 55 °C

2: 70 percent / Et₃N / methanol / 24 h / 20 °C

With borane-THF; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1055/s-2005-869989