{2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

Base Information

Chemical Name:{2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester
CAS No.:155854-10-7
Molecular Formula:C₁₉H₂₃NO₄
Molecular Weight:329.396
Hs Code.:

Synonyms:{2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

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Chemical Property of {2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

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Technology Process of {2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

There total 4 articles about {2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35718-08-2
propargyl chloroformate

: 2-<4-(2-aminoethoxy)benzyl>cyclohexan-1-one hydrochloride

: 155854-10-7
{2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

Guidance literature:: With sodium hydroxide; In water; benzene; Yield given; Ambient temperature;
DOI:10.1002/hlca.19940770218

Reference yield:

: 35718-08-2
propargyl chloroformate

: 155854-14-1
2-<4-(2-aminoethoxy)benzyl>cyclohexan-1-one

: 155854-10-7
{2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

Guidance literature:: With sodium hydroxide; In water; benzene; Yield given; Ambient temperature;
DOI:10.1002/hlca.19940770218

Reference yield:

: 22081-10-3
2-(4-Hydroxybenzyl)-1-cyclohexanone

: 155854-10-7
{2-[4-(2-Oxo-cyclohexylmethyl)-phenoxy]-ethyl}-carbamic acid prop-2-ynyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaOH / H₂O / 6 h / Heating

2: 88 percent / NH₃ / tetrahydrofuran / -78 deg C to room t.

3: 45percent NaOH / benzene; H₂O / Ambient temperature

With sodium hydroxide; ammonia; In tetrahydrofuran; water; benzene;
DOI:10.1002/hlca.19940770218