6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

Base Information

Chemical Name:6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine
CAS No.:99877-36-8
Molecular Formula:C₂₂H₂₃ClN₄O
Molecular Weight:394.904
Hs Code.:

Synonyms:6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

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Chemical Property of 6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

Chemical Property:

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Technology Process of 6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

There total 6 articles about 6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99877-28-8
5-[4-(2-Methoxy-phenyl)-piperazin-1-ylmethyl]-6-phenyl-2H-pyridazin-3-one

: 99877-36-8
6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

Guidance literature:: With trichlorophosphate; at 0 ℃;

Reference yield:

: 35386-24-4
1-(2-Methoxyphenyl)piperazine

: 99877-36-8
6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 3 h / Heating

2: 50 percent / 98 percent hydrazine hydrate / ethanol / 2 h / Heating

3: 1.) bromine; 2.) 25 percent NH₄OH / 1.) glacial acetic acid, 2 h, 60-70 deg C

4: POCl₃ / 0 °C

With ammonium hydroxide; bromine; hydrazine hydrate; trichlorophosphate; In ethanol; benzene;

Reference yield:

: 99877-45-9
β-benzoyl-γ-bromobutyric acid methyl ester

: 99877-36-8
6-Chloro-4-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-3-phenyl-pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 3 h / Heating

2: 50 percent / 98 percent hydrazine hydrate / ethanol / 2 h / Heating

3: 1.) bromine; 2.) 25 percent NH₄OH / 1.) glacial acetic acid, 2 h, 60-70 deg C

4: POCl₃ / 0 °C

With ammonium hydroxide; bromine; hydrazine hydrate; trichlorophosphate; In ethanol; benzene;