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Technology Process of (CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

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  • Chemical Name:(CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH
  • CAS No.:1355342-53-8
  • Molecular Formula:C64H63BN6O16
  • Molecular Weight:1183.05
  • Hs Code.:
(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OH)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)C(O)C<sub>6</sub>H<sub>4</sub>C<sub>13</sub>H<sub>6</sub>O<sub>2</sub>OH

Synonyms:(CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

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Chemical Property of (CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH
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Technology Process of (CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

There total 2 articles about (CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OCH<sub>2</sub>CHCH<sub>2</sub>)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)C(O)C<sub>6</sub>H<sub>4</sub>C<sub>13</sub>H<sub>6</sub>O<sub>2</sub>OH
1355342-65-2

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OH)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)C(O)C<sub>6</sub>H<sub>4</sub>C<sub>13</sub>H<sub>6</sub>O<sub>2</sub>OH
1355342-53-8

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

Guidance literature:
With tetrakis(triphenylphosphine) palladium(0); tri-n-butyl-tin hydride; acetic acid; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c1ob06667f

Reference yield: 65.0%

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OCH<sub>2</sub>CHCH<sub>2</sub>)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)C(O)C<sub>6</sub>H<sub>4</sub>C<sub>13</sub>H<sub>6</sub>O<sub>2</sub>OH
1355342-65-2

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

tri-n-butyl-tin hydride
688-73-3

tri-n-butyl-tin hydride

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OH)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)C(O)C<sub>6</sub>H<sub>4</sub>C<sub>13</sub>H<sub>6</sub>O<sub>2</sub>OH
1355342-53-8

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

Guidance literature:
With tetrakis(triphenylphosphine)palladium; acetic acid; In tetrahydrofuran; 15 min;
DOI:10.1039/c1ob06667f

Reference yield:

(CH<sub>3</sub>)4C<sub>2</sub>O<sub>2</sub>BC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>2</sub>(C(O)OH)(CH<sub>2</sub>OC(O)OCH<sub>2</sub>CH<sub>2</sub>N(C<sub>2</sub>H<sub>5</sub>)C<sub>6</sub>H<sub>4</sub>NNC<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>)CH<sub>2</sub>OC(O)N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)C(O)C<sub>6</sub>H<sub>4</sub>C<sub>13</sub>H<sub>6</sub>O<sub>2</sub>OH
1355342-53-8

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OH)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

C<sub>24</sub>H<sub>22</sub>N<sub>2</sub>O<sub>4</sub>
1355342-55-0

C24H22N2O4

disperse red 1
2872-52-8

disperse red 1

Guidance literature:
With dihydrogen peroxide; pH=8.2; aq. buffer;
DOI:10.1039/c1ob06667f
upstream raw materials:

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)N(CH3)CH2CH2N(CH3)C(O)C6H4C13H6O2OH

tri-n-butyl-tin hydride

Downstream raw materials:

(CH3)4C2O2BC6H4CH2OC6H2(C(O)OCH2CHCH2)(CH2OC(O)OCH2CH2N(C2H5)C6H4NNC6H4NO2)CH2OC(O)OC6H4NO2

C24H22N2O4

disperse red 1

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