N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide

Base Information

• Chemical Name: N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide
• CAS No.: 1246736-87-7
• Molecular Formula: Br*C₂₁H₂₈NO₂
• Molecular Weight: 406.363

Synonyms:N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide

Chemical Property of N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide

Chemical Property:

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Technology Process of N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide

There total 1 articles about N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-(bromomethyl)-5-(tert-butyl)-2-hydroxybenzaldehyde (367965-70-6) + N,N'-dimethylbenzylamine (103-83-3) → N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide (1246736-87-7)

Guidance literature:

In acetonitrile; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1039/c6cc09774j

Reference yield: 92.0%

N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide (1246736-87-7) + (S,S)-1,2-diaminocyclohexane (21436-03-3) → 1,1'-(((1E,1E')-(((1S,2S)-cyclohexane1,2-diyl)bis(azanylylidene))bis(methanylylidene))bis(5-(tert-butyl)-2-hydroxy-3,1-phenylene))bis(N-benzyl-N,N-dimethyl methanammonium)bromide

Guidance literature:

In ethanol; for 24h; Molecular sieve; Inert atmosphere;

DOI:10.1002/anie.201612493

Reference yield: 91.0%

N-benzyl-1-(5-(tert-butyl)-3-formyl-2-hydroxyphenyl)-N,N-dimethylmethylammonium bromide (1246736-87-7) + (S,S)-1,2-diaminocyclohexane (21436-03-3) → (S,S)-(+)-N,N'-bis(3-tert-butyl-5-((N-benzyl-N,N-dimethyl)-1-ylmethyl)salicylidene)-1,2-cyclohexanediamine dibromide

Guidance literature:

In ethanol; at 20 ℃; for 14h;

DOI:10.1002/chem.201000840

upstream raw materials:

3-(bromomethyl)-5-(tert-butyl)-2-hydroxybenzaldehyde

N,N'-dimethylbenzylamine

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