Technology Process of C28H38N2O5
There total 3 articles about C28H38N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 48h;
Inert atmosphere;
DOI:10.1002/chem.201201415
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; sodium hydroxide / 1,4-dioxane / 24 h
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
1,4-dioxane; dichloromethane;
DOI:10.1002/chem.201201415
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetonitrile / 4 h / 20 °C / Inert atmosphere
2: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere
With
potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetonitrile;
DOI:10.1002/chem.201201415
