(4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

Base Information

Chemical Name:(4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride
CAS No.:1620963-16-7
Molecular Formula:C₃₃H₄₃N₂*Cl
Molecular Weight:503.171
Hs Code.:

Synonyms:(4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

Chemical Property:

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Technology Process of (4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

There total 4 articles about (4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1620963-09-8
(4R,5R)-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazoline

: 100-44-7
benzyl chloride

: 1620963-16-7
(4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

Guidance literature:: In dichloromethane; at 60 ℃; for 15h; Sealed tube;
DOI:10.1055/s-0033-1338564

Reference yield:

: 60973-62-8
2,2'-(bromomethylene)bis(methylbenzene)

: 1620963-16-7
(4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 48 h / 100 °C / Sealed tube

2: dichloromethane / 15 h / 60 °C / Sealed tube

With potassium carbonate; In dichloromethane; acetone;
DOI:10.1055/s-0033-1338564

Reference yield:

: 2845-91-2
bis(2-methylphenyl)methanol

: 1620963-16-7
(4R,5R)-3-benzyl-4,5-di(tert-butyl)-1-(bis(2-methylphenyl)methyl)imidazolidinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / dichloromethane / 15 h / 0 - 20 °C

2: potassium carbonate / acetone / 48 h / 100 °C / Sealed tube

3: dichloromethane / 15 h / 60 °C / Sealed tube

With phosphorus tribromide; potassium carbonate; In dichloromethane; acetone;
DOI:10.1055/s-0033-1338564