Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)- (9CI)
CAS No.:23657-28-5
Molecular Formula:C₇H₁₂S₂
Molecular Weight:160.304
Hs Code.:
Mol file:23657-28-5.mol

Synonyms:2,3-Norbornanedithiol,cis-exo- (8CI); Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)-;2-exo,3-exo-Norbornanedithiol

Suppliers and Price of Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)- (9CI)

Chemical Property:

PSA：77.60000
LogP:2.01310

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)- (9CI)

There total 5 articles about Bicyclo[2.2.1]heptane-2,3-dithiol, (exo,exo)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 23657-27-4
exo-3,4,5-trithiatricyclo[5.2.1.0^2,6]decane

: 23657-28-5
Bicyclo<2.2.1>hepta-exo-cis-2,3-dithiol

Guidance literature:: exo-3,4,5-trithiatricyclo[5.2.1.0^2,6]decane; With lithium triethylborohydride; In tetrahydrofuran; at 65 ℃; for 2h;

With water; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.07.161

Reference yield:

: 56904-67-7,96614-16-3
bicyclo<2.2.1>heptane-cis-2,3-dithiol thionocarbonates

: 23657-28-5,96556-88-6,133209-22-0
cis-bicyclo<2.2.1>heptane-2,3-dithiol

Guidance literature:: With sodium hydroxide; In methanol; water; for 20h; Heating;
DOI:10.1021/ja00300a016

Reference yield:

: 5024-92-0
2-morpholinobicyclo<2.2.1>hept-2-en

: 23657-28-5,96556-88-6,133209-22-0
cis-bicyclo<2.2.1>heptane-2,3-dithiol

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N

2: NaOH / methanol; H₂O / 20 h / Heating

With sodium hydroxide; triethylamine; In methanol; water;
DOI:10.1021/ja00300a016