Technology Process of C38H41F6N5O4
There total 5 articles about C38H41F6N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; butan-1-ol;
at 65 ℃;
for 15h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
1.2: 15 h
2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / 0 - 20 °C
2.2: 72 h / 0 - 20 °C
3.1: hydrogen / palladium on carbon / ethanol / 24 h / 2585.81 Torr
4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 °C
5.1: N-ethyl-N,N-diisopropylamine; 1,2-dichloro-ethane / butan-1-ol; dichloromethane / 15 h / 65 °C / Sealed tube
With
hydrogenchloride; hydrogen; sodium hexamethyldisilazane; potassium hexamethylsilazane; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine;
palladium on carbon;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / 0 - 20 °C
1.2: 72 h / 0 - 20 °C
2.1: hydrogen / palladium on carbon / ethanol / 24 h / 2585.81 Torr
3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 1 h / 0 °C
4.1: N-ethyl-N,N-diisopropylamine; 1,2-dichloro-ethane / butan-1-ol; dichloromethane / 15 h / 65 °C / Sealed tube
With
hydrogenchloride; hydrogen; potassium hexamethylsilazane; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine;
palladium on carbon;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; butan-1-ol;