C₁₈H₁₂BrNO₃S

Base Information

Chemical Name:C₁₈H₁₂BrNO₃S
CAS No.:342780-76-1
Molecular Formula:C₁₈H₁₂BrNO₃S
Molecular Weight:402.268
Hs Code.:

C<sub>18</sub>H<sub>12</sub>BrNO<sub>3</sub>S

Synonyms:C₁₈H₁₂BrNO₃S

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Chemical Property of C₁₈H₁₂BrNO₃S

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Technology Process of C₁₈H₁₂BrNO₃S

There total 3 articles about C₁₈H₁₂BrNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 67216-64-2
4-Brom-N-p-toluolsulfonyl-1-naphthylamin

: 342780-76-1
C₁₈H₁₂BrNO₃S

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 16h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ol2023856

Reference yield:

: 2298-07-9
4-Bromo-1-naphthylamine

: 342780-76-1
C₁₈H₁₂BrNO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 12 h / Reflux

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate / N,N-dimethyl-formamide / 16 h / 100 °C / 760.05 Torr / Inert atmosphere

With pyridine; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate; In N,N-dimethyl-formamide;
DOI:10.1021/ol2023856

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 342780-76-1
C₁₈H₁₂BrNO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 12 h / Reflux

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate / N,N-dimethyl-formamide / 16 h / 100 °C / 760.05 Torr / Inert atmosphere

With pyridine; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; oxygen; copper diacetate; In N,N-dimethyl-formamide;
DOI:10.1021/ol2023856