ytrrium tetrahydridoborate

Base Information

• Chemical Name: ytrrium tetrahydridoborate
• CAS No.: 72033-96-6
• Molecular Formula: 3BH₄*Y
• Molecular Weight: 133.434

Synonyms:ytrrium tetrahydridoborate

Chemical Property of ytrrium tetrahydridoborate

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Technology Process of ytrrium tetrahydridoborate

There total 1 articles about ytrrium tetrahydridoborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

sodium yttrium hydroborate*4 1,2-dimethoxyethane + 3-ethylpentan-3-ol (597-49-9) → sodium tetrahydroborate (16940-66-2) + ytrrium tetrahydridoborate (72033-96-6) + bis(3-ethyl-3-pentoxy)borane (144782-40-1)

Guidance literature:

In tetrahydrofuran; byproducts: H2; under inert atm.; excess of alcohol in THF added dropwise at room temp. to stirred soln. of tetrahydroborate complex in THF (accompanied by vigorous gas evolution); stirring was continued for 1 h; mixt. allowed to stand for the reaction to be completed; within 5 ds ppt. sepd. by filtration (identified as NaBH4 by X-ray diffraction and IR spectroscopy); filtrate was distd. (vac., 0.1 mmHg) at room temp. to remove solvent and at 50°C; residue pumped out at 100-115°C; volatile collected ...;

upstream raw materials:

3-ethylpentan-3-ol

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