C₃₁H₄₅NO₇Si

Base Information Edit

Chemical Name:C₃₁H₄₅NO₇Si
CAS No.:534602-90-9
Molecular Formula:C₃₁H₄₅NO₇Si
Molecular Weight:571.786
Hs Code.:
Mol file:534602-90-9.mol

C<sub>31</sub>H<sub>45</sub>NO<sub>7</sub>Si

Synonyms:C₃₁H₄₅NO₇Si

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Chemical Property of C₃₁H₄₅NO₇Si Edit

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Technology Process of C₃₁H₄₅NO₇Si

There total 3 articles about C₃₁H₄₅NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 224192-24-9
methyl (2S)-2-{(tert-butoxy)-N-[(tert-butyl)oxycarbonyl]carbonylamino}-4-hydroxybutanoate

: 534602-90-9
C₃₁H₄₅NO₇Si

Guidance literature:: With triethylamine; at 20 ℃; for 8h;
DOI:10.1016/S0960-894X(02)01026-0

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 534602-90-9
C₃₁H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane / Inert atmosphere

1.2: Inert atmosphere

1.3: Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / 1 - 40 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With 1H-imidazole; chloro-trimethyl-silane; diisobutylaluminium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/acs.jnatprod.0c00921

Reference yield:

: 219617-08-0
dimethyl (2S)-2-{(tert-butoxy)-N-[(tert-butyl)oxycarbonyl]carbonylamino}butanedioate

: 534602-90-9
C₃₁H₄₅NO₇Si

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / 1 - 40 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With 1H-imidazole; diisobutylaluminium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/acs.jnatprod.0c00921