2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

Base Information

Chemical Name:2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol
CAS No.:1565796-96-4
Molecular Formula:C₁₈H₁₆N₂OS
Molecular Weight:308.404
Hs Code.:

Synonyms:2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

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Chemical Property of 2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

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Technology Process of 2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

There total 3 articles about 2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1565797-69-4
C₂₈H₃₂N₂O₅S

: 1565796-96-4
2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;

Reference yield:

: 1565797-68-3
C₁₃H₁₅NO₃S

: 1565796-96-4
2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide / 0.17 h

1.2: 3.5 h

2.1: trifluoroacetic acid / dichloromethane / 2 h

With trifluoroacetic acid; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 68867-18-5
2-methyl-benzothiazol-6-ol

: 1565796-96-4
2-((1E,3E)-4-(4-(methylamino)phenyl)buta-1,3-dienyl)benzo[d]thiazole-6-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / N,N-dimethyl-formamide / 16 h

2.1: sodium hydroxide / N,N-dimethyl-formamide / 0.17 h

2.2: 3.5 h

3.1: trifluoroacetic acid / dichloromethane / 2 h

With triethylamine; trifluoroacetic acid; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;