C₁₇H₁₄ClNO₇

Base Information

Chemical Name:C₁₇H₁₄ClNO₇
CAS No.:1312610-57-3
Molecular Formula:C₁₇H₁₄ClNO₇
Molecular Weight:379.754
Hs Code.:

C<sub>17</sub>H<sub>14</sub>ClNO<sub>7</sub>

Synonyms:C₁₇H₁₄ClNO₇

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Chemical Property of C₁₇H₁₄ClNO₇

Chemical Property:

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Technology Process of C₁₇H₁₄ClNO₇

There total 1 articles about C₁₇H₁₄ClNO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1312610-56-2
C₉H₇BrClNO₅

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1312610-57-3
C₁₇H₁₄ClNO₇

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 80 ℃; Inert atmosphere;

Reference yield:

: 1312610-57-3
C₁₇H₁₄ClNO₇

: 1312610-72-2
C₃₆H₄₂ClN₇O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

3.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

3.2: -5 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5.1: ammonium acetate / toluene / Reflux

6.1: boron tribromide / dichloromethane / -70 - 20 °C

6.2: Cooling with ice

6.3: 3 h / 20 °C / pH 7 - 8

With oxalyl dichloride; lithium hydroxide monohydrate; ammonium acetate; water; boron tribromide; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;

Reference yield:

: 1312610-57-3
C₁₇H₁₄ClNO₇

: 1312610-73-3
C₃₆H₄₅N₇O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

3.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

3.2: -5 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5.1: ammonium acetate / toluene / Reflux

6.1: boron tribromide / dichloromethane / -70 - 20 °C

6.2: Cooling with ice

6.3: 3 h / 20 °C / pH 7 - 8

7.1: hydrogen / palladium(II) hydroxide / methanol / 24 h / 50 °C / 2585.81 Torr

With oxalyl dichloride; lithium hydroxide monohydrate; ammonium acetate; water; hydrogen; boron tribromide; N-ethyl-N,N-diisopropylamine; palladium(II) hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;