1-bromo-2,7-dicyclohexylnaphthalene

Base Information

Chemical Name:1-bromo-2,7-dicyclohexylnaphthalene
CAS No.:1286791-37-4
Molecular Formula:C₂₂H₂₇Br
Molecular Weight:371.36
Hs Code.:

Synonyms:1-bromo-2,7-dicyclohexylnaphthalene

Suppliers and Price of 1-bromo-2,7-dicyclohexylnaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-2,7-dicyclohexylnaphthalene

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Technology Process of 1-bromo-2,7-dicyclohexylnaphthalene

There total 3 articles about 1-bromo-2,7-dicyclohexylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 136288-21-6
2,7-Dicyclohexylnaphthalene

: 1286791-37-4
1-bromo-2,7-dicyclohexylnaphthalene

Guidance literature:: With bromine; In dichloromethane; at -78 ℃; regioselective reaction; Inert atmosphere;

Reference yield:

: 108-85-0
1-bromocyclohexane

: 1286791-37-4
1-bromo-2,7-dicyclohexylnaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: bromine / dichloromethane / 5 h / -78 °C / Inert atmosphere

With bromine; iodine; magnesium; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-0035-1561669

Reference yield:

: 582-17-2
2,7-Dihydroxynaphthalene

: 1286791-37-4
1-bromo-2,7-dicyclohexylnaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine; triphenylphosphine / acetonitrile / 20 - 70 °C / Inert atmosphere

2.1: iodine; magnesium / tetrahydrofuran / 60 °C / Inert atmosphere; Reflux

2.2: 20 °C / Inert atmosphere

3.1: bromine / dichloromethane / -78 °C / Inert atmosphere

With bromine; iodine; magnesium; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;