8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

Base Information

Chemical Name:8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate
CAS No.:128162-91-4
Molecular Formula:C₂₉H₄₉NO₅Si
Molecular Weight:519.797
Hs Code.:

Synonyms:8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

Suppliers and Price of 8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

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Technology Process of 8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

There total 1 articles about 8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 128114-52-3,128162-88-9,128162-89-0,128162-90-3,133006-61-8
(-)-8-Phenylmenthyl 2-Hydroxy-5-methyl-3-nitro-hexanoate

: 128162-94-7
8-Phenylmenthyl (2R,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

: 128162-95-8
8-Phenylmenthyl (2R,3R)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

: 128162-91-4
8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

: 128114-53-4
8-Phenylmenthyl (2S,3R)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00302a050

Reference yield:

: 128162-91-4
8-Phenylmenthyl (2S,3S)-5-Methyl-3-nitro-2-((triethylsilyl)oxy)hexanoate

: 65253-04-5
(-)-8-phenylmenthol

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Raney Ni / ethanol / 16 h / 50 °C / 30400 Torr

2: methylammonium fluoride (MAF) / acetonitrile; tetrahydrofuran

3: 60 percent / 6N-aq. HCl

With hydrogenchloride; hydrogen; methylammmonium fluoride; nickel; In tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/jo00302a050