C₂₇H₂₉N₅O₂

Base Information

Chemical Name:C₂₇H₂₉N₅O₂
CAS No.:1073472-92-0
Molecular Formula:C₂₇H₂₉N₅O₂
Molecular Weight:455.56
Hs Code.:

C<sub>27</sub>H<sub>29</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:C₂₇H₂₉N₅O₂

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Chemical Property of C₂₇H₂₉N₅O₂

Chemical Property:

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Technology Process of C₂₇H₂₉N₅O₂

There total 6 articles about C₂₇H₂₉N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 1073472-76-0
C₂₂H₂₀N₄O

: 1538-75-6
2,2-dimethylpropanoic anhydride

: 1073472-92-0
C₂₇H₂₉N₅O₂

Guidance literature:: C₂₂H₂₀N₄O; With hydroxylamine hydrochloride; potassium carbonate; In ethanol; for 16h; Heating / reflux;

2,2-dimethylpropanoic anhydride; at 0 ℃; for 3h; Heating / reflux;

Reference yield:

: 52763-21-0
ethyl 1-benzyl-3-oxopiperidine-4-carboxylate hydrochloride

: 1073472-92-0
C₂₇H₂₉N₅O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 15 h / 20 °C / 760.05 Torr

1.2: 3 h / 20 °C

2.1: potassium carbonate / methanol; water / 15 h / 60 °C

3.1: caesium carbonate / tetrahydrofuran / 15 h / Heating / reflux

4.1: hydrogenchloride / 1,4-dioxane; ethyl acetate / 20 °C

5.1: sodium hydrogencarbonate / dichloromethane; water / 15 h / 0 °C

6.1: hydroxylamine hydrochloride; potassium carbonate / ethanol / 16 h / Heating / reflux

6.2: 3 h / 0 °C / Heating / reflux

With hydrogenchloride; hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate;

Reference yield:

: 338739-89-2
tert-butyl 4-hydroxy-2-methyl-5,6-dihydropyrido[3,4-d]pyrimidine-7(8H)-carboxylate

: 1073472-92-0
C₂₇H₂₉N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / tetrahydrofuran / 15 h / Heating / reflux

2.1: hydrogenchloride / 1,4-dioxane; ethyl acetate / 20 °C

3.1: sodium hydrogencarbonate / dichloromethane; water / 15 h / 0 °C

4.1: hydroxylamine hydrochloride; potassium carbonate / ethanol / 16 h / Heating / reflux

4.2: 3 h / 0 °C / Heating / reflux

With hydrogenchloride; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; ethyl acetate;