C₃₃H₄₂N₈O₁₁

Base Information

Chemical Name:C₃₃H₄₂N₈O₁₁
CAS No.:1415917-82-6
Molecular Formula:C₃₃H₄₂N₈O₁₁
Molecular Weight:726.743
Hs Code.:

C<sub>33</sub>H<sub>42</sub>N<sub>8</sub>O<sub>11</sub>

Synonyms:C₃₃H₄₂N₈O₁₁

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Chemical Property of C₃₃H₄₂N₈O₁₁

Chemical Property:

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Technology Process of C₃₃H₄₂N₈O₁₁

There total 10 articles about C₃₃H₄₂N₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1415917-81-5
C₂₀H₂₄N₄O₇

: 1415917-80-4
C₁₃H₂₀N₄O₅

: 1415917-82-6
C₃₃H₄₂N₈O₁₁

Guidance literature:: C₂₀H₂₄N₄O₇; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 1h;

C₁₃H₂₀N₄O₅; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc36566a

Reference yield:

: 14260-27-6
3-deoxy-3-iodo-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 1415917-82-6
C₃₃H₄₂N₈O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium azide / N,N-dimethyl-formamide / 105 °C

2.1: palladium 10% on activated carbon

3.1: sodium hydrogencarbonate / water; methanol

4.1: water; acetic acid

5.1: sodium periodate / water; methanol

6.1: potassium carbonate / methanol

7.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol

8.1: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 760.05 Torr

9.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 0 °C

10.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

10.2: 24 h / 20 °C / Inert atmosphere

With sodium periodate; sodium azide; copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; acetic acid; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1039/c2cc36566a

Reference yield:

: 3-amino-3-deoxy-1,2:5,6-di-O-isopropylidene-D-glucofuranose

: 1415917-82-6
C₃₃H₄₂N₈O₁₁

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate / water; methanol

2.1: water; acetic acid

3.1: sodium periodate / water; methanol

4.1: potassium carbonate / methanol

5.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol

6.1: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 760.05 Torr

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 °C

7.2: 24 h / 20 °C / Inert atmosphere

With sodium periodate; copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; acetic acid; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1039/c2cc36566a