N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide

Base Information

• Chemical Name: N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide
• CAS No.: 1206701-65-6
• Molecular Formula: C₂₈H₂₆N₄O₄
• Molecular Weight: 482.539

Synonyms:N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide

Chemical Property of N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide

Chemical Property:

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Technology Process of N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide

There total 1 articles about N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-chloro-N2,N6-bis[(1R)-2-hydroxy-1-phenylethyl]pyridine-2,6-dicarboxamide (1082739-11-4) + 4-pyridylboronic acid (1692-15-5) → N2,N6-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide (1206701-65-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 48h; Inert atmosphere;

DOI:10.1002/hlca.200900087

Reference yield: 92.0%

N2,N6-bis[(1R)-2-hydroxy-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide (1206701-65-6) → N2,N6-bis[(1R)-2-chloro-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide (1206701-66-7)

Guidance literature:

With thionyl chloride; for 7h; Reflux;

DOI:10.1002/hlca.200900087

upstream raw materials:

4-chloro-N²,N⁶-bis[(1R)-2-hydroxy-1-phenylethyl]pyridine-2,6-dicarboxamide

4-pyridylboronic acid

Downstream raw materials:

N²,N⁶-bis[(1R)-2-chloro-1-phenylethyl][4,4'-bipyridine]-2,6-dicarboxamide

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