Technology Process of 1-chloro-2-methoxy-4-(2-nitrovinyl)benzene
There total 5 articles about 1-chloro-2-methoxy-4-(2-nitrovinyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methylamine hydrochloride; sodium carbonate;
In
ethanol;
for 72h;
Ambient temperature;
DOI:10.1021/jm00101a018
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / K2CO3 / acetone
2: 92 percent / KMnO4 / pyridine; H2O / 1.) 50 deg C, 24 h, 2.) RT, 13 h
3: 82 percent / LiAlH4 / diethyl ether; dioxane
4: 93 percent / pyridinium chlorochromate / CH2Cl2
5: 89 percent / CH3NH2*HCl, Na2CO3 / ethanol / 72 h / Ambient temperature
With
potassium permanganate; lithium aluminium tetrahydride; methylamine hydrochloride; sodium carbonate; potassium carbonate; pyridinium chlorochromate;
In
1,4-dioxane; pyridine; diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1021/jm00101a018
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 93 percent / pyridinium chlorochromate / CH2Cl2
2: 89 percent / CH3NH2*HCl, Na2CO3 / ethanol / 72 h / Ambient temperature
With
methylamine hydrochloride; sodium carbonate; pyridinium chlorochromate;
In
ethanol; dichloromethane;
DOI:10.1021/jm00101a018
