C₃₅H₃₂INO₄

Base Information

Chemical Name:C₃₅H₃₂INO₄
CAS No.:1395877-66-3
Molecular Formula:C₃₅H₃₂INO₄
Molecular Weight:657.548
Hs Code.:

C<sub>35</sub>H<sub>32</sub>INO<sub>4</sub>

Synonyms:C₃₅H₃₂INO₄

Suppliers and Price of C₃₅H₃₂INO₄

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Chemical Property of C₃₅H₃₂INO₄

Chemical Property:

Purity/Quality:

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Technology Process of C₃₅H₃₂INO₄

There total 1 articles about C₃₅H₃₂INO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1395877-06-1
C₄₃H₃₉NO₆

: 1395877-66-3
C₃₅H₃₂INO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; water / isopropyl alcohol / 3 h / Reflux

2.1: triethylamine; diphenylphosphoranyl azide / toluene / 2 h / 20 °C

2.2: 2 h / 70 °C

2.3: 3 h / Reflux

3.1: hydrogenchloride; sodium nitrite / acetonitrile; water / 0.5 h / 0 - 5 °C

3.2: 6 h / 20 °C

With hydrogenchloride; diphenylphosphoranyl azide; water; triethylamine; sodium hydroxide; sodium nitrite; In water; isopropyl alcohol; toluene; acetonitrile;

Reference yield: 58.0%

: 14376-79-5
3,3,5,5-tetramethylcyclohexanone

: 1395877-66-3
C₃₅H₃₂INO₄

: 1395877-67-4
C₄₅H₅₁NO₅

Guidance literature:: C₃₅H₃₂INO₄; With n-butyllithium; In hexane; toluene; at -50 ℃; for 0.5h;

3,3,5,5-tetramethylcyclohexanone; In hexane; toluene; at 0 ℃; for 3h;

With water; In hexane; toluene;

Reference yield:

: 1395877-66-3
C₃₅H₃₂INO₄

: 1395877-68-5
C₃₈H₄₅NO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / toluene; hexane / 0.5 h / -50 °C

1.2: 3 h / 0 °C

2.1: ammonium formate / 5%-palladium/activated carbon / tetrahydrofuran / 8 h / 20 °C

With n-butyllithium; ammonium formate; 5%-palladium/activated carbon; In tetrahydrofuran; hexane; toluene;