3-(2,4-dimethylphenyl)anthranil

Base Information

• Chemical Name: 3-(2,4-dimethylphenyl)anthranil
• CAS No.: 87895-73-6
• Molecular Formula: C₁₅H₁₃NO
• Molecular Weight: 223.274
• Mol file: 87895-73-6.mol

Synonyms:3-(2,4-dimethylphenyl)anthranil

Chemical Property of 3-(2,4-dimethylphenyl)anthranil

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2,4-dimethylphenyl)anthranil

There total 5 articles about 3-(2,4-dimethylphenyl)anthranil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2,4-dimethyl-2'-nitro-benzophenone (143824-86-6) → 3-(2,4-dimethylphenyl)anthranil (87895-73-6)

Guidance literature:

With indium; iodine; In methanol; at 50 ℃; for 6h;

DOI:10.1016/j.tetlet.2006.08.027

Reference yield: 84.0%

(2-Azido-phenyl)-(2,4-dimethyl-phenyl)-methanone (87895-66-7) → 3-(2,4-dimethylphenyl)anthranil (87895-73-6)

Guidance literature:

In various solvent(s); Heating;

Reference yield:

2-methyl-4-oxo-3,1-benzoxazine (525-76-8) → 3-(2,4-dimethylphenyl)anthranil (87895-73-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) magnesium / 1.) ether, 2.) ice-bath, 4 h

2: 1.) conc. HCl, sodium nitrite, 2.) sodium azide, sodium acetate / 1.) acetic acid, water, below 5 deg C

3: 83 percent / various solvent(s) / 3 h / Heating

With hydrogenchloride; sodium azide; sodium acetate; magnesium; sodium nitrite; In various solvent(s);

upstream raw materials:

(2-Azido-phenyl)-(2,4-dimethyl-phenyl)-methanone

2,4-dimethyl-2'-nitro-benzophenone

2-methyl-4-oxo-3,1-benzoxazine

2-amino-2',4'-dimethylbenzophenone

Downstream raw materials:

2,4-dimethylacridone

2-amino-2',4'-dimethylbenzophenone