Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester
CAS No.:173725-90-1
Molecular Formula:C₆₆H₆₅ClO₁₅S
Molecular Weight:1165.75
Hs Code.:

Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Synonyms:Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Suppliers and Price of Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

There total 3 articles about Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 173725-89-8
benzyl 2-O-benzoyl-6-O-benzyl-3-O-chloroacetyl-α-D-glucopyranoside

: 173725-87-6
phenyl 3,4,6-tri-O-benzyl-2-(3-hydroxycarbonyl)propionyl-1-thio-α-D-mannopyranoside

: 173725-90-1
Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 25 ℃; for 5h;
DOI:10.1016/0040-4039(95)01952-E

Reference yield:

: 127299-77-8
phenyl 3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 173725-90-1
Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / DMAP / pyridine / 24 h / 25 °C

2: 52 percent / DCC / CH₂Cl₂ / 5 h / 25 °C

With dmap; dicyclohexyl-carbodiimide; In pyridine; dichloromethane;
DOI:10.1016/0040-4039(95)01952-E

Reference yield:

: benzyl 2-O-benzoyl-4,6-O-benzylidene-3-O-chloroacetyl-α-D-glucopyranoside

: 173725-90-1
Succinic acid (2R,3R,4S,5R,6S)-5-benzoyloxy-6-benzyloxy-2-benzyloxymethyl-4-(2-chloro-acetoxy)-tetrahydro-pyran-3-yl ester (2R,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NaCNBH₃, HCl / tetrahydrofuran; diethyl ether / 0.5 h / 25 °C

2: 52 percent / DCC / CH₂Cl₂ / 5 h / 25 °C

With hydrogenchloride; sodium cyanoborohydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/0040-4039(95)01952-E